Synthesis,Characterization and Crystal Structure of 4,5-Bis(Cyclohexanecarbonylthio)-1,3-dithiolane-2-thione Crystal |
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| Authors: | Yan Ling Wang Mei Li Jun Yao Ye Fei Wang Jing Jing Zheng Li Ma |
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| Institution: | (1) School of Petroleum Engineering, China University of Petroleum (East China), 266555 Qingdao, People’s Republic of China;(2) Material Science and Engineering of Shandong Institute of Light Industry, 250353 Jinan, People’s Republic of China |
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| Abstract: | Abstract A new crystal of 4,5-bis(cyclohexanecarbonylthio)-1,3-dithiolane-2-thione has been prepared at room temperature and characterized
by elemental analysis, UV–Vis–NIR absorption spectrum and X-ray single crystal determination. The complex crystallized in
triclinic space group P-1 with unit cell dimensions a = 5.37370(10) ?, b = 12.8618(2) ?, c = 15.2481(2) ?, α = 74.8530(10)°, β = 80.6000(10)°, γ = 85.9550(10)°, V = 1003.18(3) ?3, Z = 2, D
x = 1.3861(1) g cm−3. The X-ray structure determination revealed that the crystal is centered-symmetrical and the molecules form dimers with a
long intermolecular S···S interaction in the crystal. |
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