| 胭脂树低聚糖的结构分析 |
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| 引用本文： | 任风芝,陈书红,张雪霞,李丽红,高月麒,王宁.胭脂树低聚糖的结构分析[J].波谱学杂志,2011,28(1):160-167. |
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| 作者姓名： | 任风芝 陈书红 张雪霞 李丽红 高月麒 王宁 |
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| 作者单位： | 华北制药集团 新药研究开发有限责任公司，微生物药物国家研究工程中心，河北 石家庄 050015 |
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| 摘 要： | 从胭脂树（Bixo orellana）种子中分离得到了一种胭脂树低聚糖：α-D-半乳糖-(1→3)-α-D-半乳糖-(1→6) -α-D-葡萄糖-(1→2)-β-D-果糖（BO-1）. 通过1D NMR和2D NMR实验技术对其1H NMR和13C NMR谱信号进行了全归属.
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| 关 键 词： | 核磁共振（NMR） 胭脂树种子 胭脂树低聚糖 归属 |
| 收稿时间： | 2010-03-19 |
| 修稿时间： | 2010-05-14 |
Structure Analysis of an Oligosaccharide Isolated from Bixo orellana by NMR Spectroscopy |
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| REN Feng-zhi,CHEN Shu-hong,ZHANG Xue-xia,LI Li-hong,GAO Yue-qi,WANG Ning.Structure Analysis of an Oligosaccharide Isolated from Bixo orellana by NMR Spectroscopy[J].Chinese Journal of Magnetic Resonance,2011,28(1):160-167. |
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| Authors: | REN Feng-zhi CHEN Shu-hong ZHANG Xue-xia LI Li-hong GAO Yue-qi WANG Ning |
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| Institution: | New Drug Research and Development Center, North China Pharmaceutical Group Corporation, National Microbial Medicine Engineering and Research Center, Shijiazhuang 050015, China |
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| Abstract: | An oligosaccharide, α-D-Gal-(1→3)-α-D-Gal-(1→6)-α-D-Glc-(1→2)-β-D-Fru (BO-1), was isolated from the seed of Bixo orellana. The 13C and 1H NMR chemical shifts of the compound were assigned by 1D and 2D NMR techniques, including COSY、HMQC and HMBC. |
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| Keywords: | NMR Bixo orellana oligosaccharide chemical shift assignment |
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