Bisthiourea: thermal and structural investigation |
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| Authors: | Pramod B Pansuriya Hitesh M Parekh Holger B Friedrich Glenn E M Maguire |
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| Institution: | 1. School of Chemistry, University of KwaZulu-Natal, Westville Campus, Durban, 4000, South Africa
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| Abstract: | Bisthiourea derivatives 1,1′-(ethane-1,2-diyl)bis(3-phenylthiourea), 1,1′-(propane-1,3-diyl)bis(3-phenylthiourea), and 1,1′-(butane-1,4-diyl)bis(3-phenylthiourea) have been synthesized and characterized by IR, 1H NMR, and 13C NMR. Suitable crystals of 1,1′-(propane-1,3-diyl)bis(3-phenylthiourea) were grown for single-crystal X-ray analysis and from the data it was observed that they organize into the P-1 space group. The thermal decomposition of these compounds has been studied by TG–DSC. |
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