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MIP—AAS测镍时2种放电—吸收管性能的比较
引用本文:段忆翔,杜朝晖.MIP—AAS测镍时2种放电—吸收管性能的比较[J].高等学校化学学报,1992,13(9):1176-1179.
作者姓名:段忆翔  杜朝晖
作者单位:吉林大学化学系 长春130023 (段忆翔,杜朝晖,侯明轶,刘军),吉林大学化学系 长春130023(金钦汉)
摘    要:本文以镍为例,分别对MIP-AAS中所使用的T形和L形2种放电-吸收管的性能进行了详细的比较研究。讨论了各种实验参数对不同放电-吸收管的影响差异,从中总结出了一些初步的经验规律.

关 键 词:放电-吸收管    MIP-AAS

Performance Comparison Between Two Different Absorption Cells Used in MIP-AAS for Determination of Nickel
DUAN Yi-Xiang DU Zhao-Hui,HOU Ming-Yi,LIU Jun,JIN Qin-Han.Performance Comparison Between Two Different Absorption Cells Used in MIP-AAS for Determination of Nickel[J].Chemical Research In Chinese Universities,1992,13(9):1176-1179.
Authors:DUAN Yi-Xiang DU Zhao-Hui  HOU Ming-Yi  LIU Jun  JIN Qin-Han
Abstract:A systematic performance comparison between two different absorption cells used in MIP-AAS for the determination of nickel is completed in this paper.Various factors,such as microwave forward power,carrier gas flow rate,the acidity of the sample solution,etc.,which affected the absorbance,were studied and compared with each other in detail.The effects caused by easily ionized elements and some concomitant elements were also examined for this purpose.A significant enhancement in sensitivity was observed in the determination of nickel when Ca,Mg or La existed.Some conclusions about the performance of T-shaped and L-shaped absorption cells were made
Keywords:Microwave induced plasma  Atomic absorption spectrometry  Discharge-absorption cells  Determination of nickel
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