| 裂解色谱与裂解质谱对高分子分析的评价 |
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| 引用本文： | 吴万年,王复.裂解色谱与裂解质谱对高分子分析的评价[J].功能高分子学报,1992,5(1):11-18. |
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| 作者姓名： | 吴万年 王复 |
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| 作者单位： | 华东化工学院分析测试中心，华东化工学院分析测试中心，华东化工学院分析测试中心，华东化工学院分析测试中心 上海 200237，上海 200237，上海 200237，上海 200237 |
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| 摘 要： | 本文报导了在日立 M-80型气相色谱/质谱仪上装上CDS Pyroprobe 100型裂解器,组成既能做裂解色谱/质谱(Py-GC/MS),又能做裂解质谱(Py-MS)的分析裂解系统,通过对一系列的高分子裂解试验,评价了二者的性能。
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| 关 键 词： | 分析裂解 裂解色谱 裂解质谱 |
Evaluation of Py-GC and Py-MS for Analysis of High Polymers |
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| Wu Wannian,Wang Fu,Shi Xinmei,Sha Huixin Analysis and Rescarch Center.,East China Univ of Chem. Tech.,Shanghai.Evaluation of Py-GC and Py-MS for Analysis of High Polymers[J].Journal of Functional Polymers,1992,5(1):11-18. |
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| Authors: | Wu Wannian Wang Fu Shi Xinmei Sha Huixin Analysis and Rescarch Center East China Univ of Chem Tech Shanghai |
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| Institution: | Wu Wannian,Wang Fu,Shi Xinmei,Sha Huixin Analysis and Rescarch Center.,East China Univ of Chem. Tech.,Shanghai 200237 |
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| Abstract: | In this work, first a new analytical pyrolysis system was developed by incorpo-rating pyrolysis--gas chromatography/ mass spectrometry with pyolysis--massspectrometry on Hitachi model M--80 doublc-focusing mass spectrometer. By this sys-tem it became possible to measure characteristic and reproducible GC pyrogram ormass pyrogram for varioug polymers. The performance of Py--GC / MS and Py--MSwasevaluated and compared. |
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| Keywords: | analytical pyrolysis pyrolysis-gas chromatography pyrolysis-mass spectrometry |
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