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Recent developments in dynamic kinetic resolution

Authors:	Hélène PellissierAuthor Vitae

Institution:	Université Paul Cézanne—Aix-Marseille III, UMR CNRS n° 6263, Equipe Chirosciences, Case 541, Avenue Esc. Normandie-Niemen, 13397 Marseille Cedex 20, France

Abstract:

Keywords:	Ac acetyl AIBN 2 2&prime -azobisisobutyronitrile Ar aryl Atm atmosphere BARF tetrakis[3 5-bis(trifluoromethyl)phenyl]borate BINAP 2 2&prime -bis(diphenylphosphanyl)-1 1&prime -binaphthyl BINOL 1 1&prime -bi-2-naphthol BIPHEP 2 2&prime -bis(diphenylphosphino)-1 1&prime -biphenyl Bn benzyl BTAH benzyltrimethylammonium hydroxide Bu butyl Bz benzoyl c cyclo Cod cyclooctadiene Cp cyclopentadienyl CPME cyclopentyl methyl ether Cy cyclohexyl DABCO 1 4-diazabicyclo[2 2 2]octane DACH 1 2-diaminocyclohexane dba (E E)-dibenzylideneacetone DBU 1 8-diazabicyclo[5 4 0]undec-7-ene de diastereomeric excess DIEA diisopropylethylamine DIFLUORPHOS 5 5&prime -bis(diphenylphosphino)-2 2 2&prime 2&prime -tetrafluoro-4 4&prime -bi-1 3-benzodioxole DKR dynamic kinetic resolution DMAPEN 2-dimethylamino-1-phenylethylamine DMF dimethylformamide DMM dimethylmethoxy dmpe 1 2-bis(dimethylphosphino)-ethane DMSO dimethylsulfoxide DPEN 1 2-diphenylethylenediamine DYKAT dynamic kinetic asymmetric transformation ee enantiomeric excess Et ethyl Fu furyl GABA γ-aminobutyric acid HEPES 4-(2-hydroxyethyl)-1-piperazineethanesulfonic acid Hex hexyl Hept heptyl L ligand LDA lithium diisopropylamide Me methyl MOM methoxymethyl Ms mesyl NADPH nicotinamide adenine dinucleotide phosphate Naph naphthyl Non nonyl Nu nucleophile Pa pascal Pent pentyl Ph phenyl PHOX phosphinooxazoline PMB p-methoxybenzoyl Pr propyl py pyridyl PYBOX 2 6-bis(2-oxazolyl)pyridine SDP spiro diphosphine SEM 2-(trimethylsilyl)ethoxymethyl TBAI tetra-n-butylammonium iodide TBDPS tert-butyldiphenylsilyl TBS tert-butyldimethylsilyl TEA triethylamine TFA trifluoroacetic acid TFE trifluoroethanol THF tetrahydrofuran Thio thiophene Tf trifluoromethanesulphonyl TMS trimethylsilyl Tol tolyl Troc 2 2 2-trichloroethoxycarbonyl Ts 4-toluenesulfonyl (tosyl)
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