Preparation of rhenium carbonyl chloride |
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Authors: | K. N. Anisimov L. I. Baryshnikov |
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Affiliation: | (1) Institute of Heteroorganic Compounds, Academy of Sciences, USSR |
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Abstract: | Summary The reaction between iron pentacarbonyl and rhenium pentachloride in ethyl ether under a pressure of hydrogen and carbon dioxide forms rhenium carbonyl chloride in 30% yield. It was not possible by this method to prepare the total-rhenium carbonyl Re2(CO)10. |
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