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Syntheses of spherical silica and titania from alkoxides on a laboratory scale
Authors:K Tani  Y Suzuki
Institution:(1) Faculty of Engineering, Yamanashi University, Takeda 4-3-11, 400 Kofu, Japan
Abstract:Summary A process to synthesize silica and titania as spherical packing materials has been investigated on the laboratory scale by the sol-gel method. The silica and titania obtained were tested under normal-phase separation conditions for comparison of their retention characteristics silica witha a commercial. The silica was found to be similar in its retention behaviour to the commercial silica. The titania showed basic properties and strongly retained acidic compounds.
Keywords:Column liquid chromatography  Column packings  Silica and titania  Sol-gel method
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