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Hydroxylamine on Clay: a Direct Synthesis of Nitriles from Aromatic Aldehydes Using Microwaves Under Solvent-Free Conditions |
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| Authors: | Rajender?S.?Varma author-information" > author-information__contact u-icon-before" > mailto:chm_rsv@shsu.edu" title=" chm_rsv@shsu.edu" itemprop=" email" data-track=" click" data-track-action=" Email author" data-track-label=" " >Email author,Kannan?P.?Naicker |
| Affiliation: | 1.Department of Chemistry,Sam Houston State University,Huntsville,USA;2.Texas Research Institute for Environmental Studies (TRIES),Sam Houston State University,Huntsville,USA |
| Abstract: | In a solvent-free system, hydroxylamine hydrochloride impregnated montmorillonite K 10 clay expeditiously converts arylaldehydes to the corresponding nitriles under microwave irradiation conditions. This rapid one-pot method produces pure products in high yields (89–95%) within 1 to 1.5 min. |
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