| 混合模板法制备螺旋纳米结构二氧化硅 |
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| 引用本文： | 彭少华,毕丽峰,陈玉霞,李艺,杨永刚,李宝宗.混合模板法制备螺旋纳米结构二氧化硅[J].化学研究,2009,20(2):17-19. |
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| 作者姓名： | 彭少华 毕丽峰 陈玉霞 李艺 杨永刚 李宝宗 |
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| 作者单位： | 苏州大学,独墅湖校区材料与化学化工学部,江苏,苏州,215123 |
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| 基金项目： | 江苏省自然科学基金，江苏高校国家级有机化学重点学科培育点经费资助项目 |
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| 摘 要： | 用凝胶剂高氯酸环（L-11-（N-甲基咪唑）十一烷基天冬酰胺-L-苯丙酰胺）（11mim ClO4）和十六烷基三甲基氯化铵（CTAC）作模板剂，经溶胶-凝胶过程，制备纳米结构二氧化硅．使用冷场发射扫描电镜（FESEM），表征了多种反应条件下样品的形貌和表面结构．结果表明，通过调节CTAC和凝胶剂的质量比，可以得到螺旋介孔二氧化硅纳米纤维，其长度为数百纳米，孔径为3．0nm．
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| 关 键 词： | 纳米带 纳米管 纳米纤维 介孔 二氧化硅 凝胶剂 |
Preparation of Helical Nanostructured Silica Using Gelator and Surfactant as Template |
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| PENG Shao-hua,BI Li-feng,CHEN Yu-xia,LI Yi,YANG Yong-gang,LI Bao-zong.Preparation of Helical Nanostructured Silica Using Gelator and Surfactant as Template[J].Chemical Research,2009,20(2):17-19. |
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| Authors: | PENG Shao-hua BI Li-feng CHEN Yu-xia LI Yi YANG Yong-gang LI Bao-zong |
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| Institution: | (College of Chemistry, Chemical Engineering and Materials Science, Suzhou University, Suzhou 215123, Jiangsu, China) |
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| Abstract: | Helical nanostructured silica was prepared by sol-gel method using a chiral cationic gelator cyclo(L-11-(N-methylimidazolium)undecylasapaginyl-L-phenylalanyl) perchlorate(11mimClO4) and cetyltrimethylammonium chloride(CTAC) as templates.Field emitted scanning electron microscopy(FESEM) was utilized to characterize the shape,size and structure of the products obtained at different reaction conditions.By controlling the mass ratio of gelator to CTAC,mesoporous helical silica nanofibers was obtained.These mesoporous silica nanofibers were hundreds nm in length and 3.0 nm in inner-pore-diameter. |
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| Keywords: | nanoribbon nanotube nanofiber mesoporous silica gelator |
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