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Application of highly sulfonated single-walled carbon nanotubes: An efficient heterogeneous catalyst for the one-pot synthesis of 14-aryl-14H-dibenzo[a,j]xanthenes under solvent-free conditions
Authors:Reza Fareghi-Alamdari  Mohsen GolestanzadehFarima Agend  Negar Zekri
Affiliation:Department of Chemistry and Chemical engineering, Malek-Ashtar University of Technology, 16765-3454 Tehran, Iran
Abstract:Highly sulfonated single-walled carbon nanotube-catalyzed synthesis of 14-aryl-14H-dibenzo[a,j]xanthenes in excellent yields and very short reaction times. Sulfonated single-walled carbon nanotubes are prepared using a chemical and simple process and it characterized by Scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FT-IR), Raman spectroscopy, Thermal gravimetric analysis (TGA) and acid-base titration. The sulfonated single-walled carbon nanotube was easily separated by simple filtration and was recycled eight consecutive times without any loss in its activity.
Keywords:Heterogeneous catalyst   Dibenzoxanthene   Carbon nanotubes   Characterization   Solid acid   Reusable catalyst
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