In-Situ SEM J-Testing and Crack-Tip Micromechanics of Zircaloy-4 by Three-Point Bending

A three-point bend fixture has been designed, fabricated, and utilized to demonstrate the feasibility of performing in-situ J-testing at ambient and elevated temperatures inside a scanning electron microscope (SEM). Using the three-point bend test technique, in-situ SEM J-testing has been performed to measure the crack mouth opening displacement and crack extension as a function of the applied load in order to generate J-R curves for Zircaloy-4 at 25°C and 316°C. Once the J-R curve is determined, an equivalent K_J-resistance (K_J-R) curve is computed on the basis of a relationship between the J-integral (J) and the stress intensity factor (K). The J-R and K_J-R curves of Zircaloy-4 exhibit a rising R-curve behavior, while the elastic K-R curve underestimates the fracture resistance of Zircaloy-4 once substantial crack extension has occurred. For the specimen dimensions considered, the J-R curves generated by in-situ SEM J-tests are not sensitive to the specimen geometry and measure the actual fracture resistance of the material. Furthermore, the onset of crack extension is dictated by the emission of one or more slipbands from the crack tip, and a change in the crack-tip displacement field, followed by void formation along the slipband, and linkage of the voids with the main crack.