| 分光光度法测定聚维酮碘中的碘 |
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| 引用本文： | 张振南,戴歌心,孙哲,王学宝.分光光度法测定聚维酮碘中的碘[J].光谱实验室,2010,27(4):1667-1670. |
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| 作者姓名： | 张振南 戴歌心 孙哲 王学宝 |
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| 作者单位： | 1. 温州医学院分析测试中心,浙江省温州市茶山高教园区中心北路3号,325035
2. 温州医学院附属第一医院,浙江省温州市,325000 |
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| 摘 要： | 建立分光光度法测定聚维酮碘溶液中碘含量的方法。在酸性条件下,利用过氧化氢溶液将聚维酮碘溶液中结合碘转化为游离碘,用二氯甲烷萃取碘,采用分光光度法进行含量测定,碘的二氯甲烷溶液在504nm处有最大吸收,有效碘浓度在0.0001—0.002mol·L-1范围内线性关系良好(r=0.9995),平均回收率(n=9)为99.48%。该方法操作简便,结果准确,重现性好,可用于聚维酮碘溶液的质量控制。
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| 关 键 词： | 分光光度法 聚维酮碘 碘 |
Determination of Iodine in Povidone Iodine Solution by Spectrophotometry |
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| ZHANG Zhen-Nan,DAI Ge-Xin,SUN Zhe,WANG Xue-Bao.Determination of Iodine in Povidone Iodine Solution by Spectrophotometry[J].Chinese Journal of Spectroscopy Laboratory,2010,27(4):1667-1670. |
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| Authors: | ZHANG Zhen-Nan DAI Ge-Xin SUN Zhe WANG Xue-Bao |
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| Institution: | ZHANG Zhen-Nan a DAI Ge-Xin b SUN Zhe a WANG Xue-Bao a(Center of Wenzhou Medical College,Wenzhou 325035,P.R.China)a(The First Affiliated Hospital of Wenzhou Medical College,Wenzhou 325000,P.R.China) |
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| Abstract: | Method for the determination of iodine from povidone iodine solution was developed by the spectrophotometry.The bound iodine in Povidone iodine solution was changed to free iodine by H2O2 in the acidic environment.Then the iodine was solved by CH2Cl2 and the content was determined by spectrophotometry.The solution of iodine solved in CH2Cl2 had max absorbance at 504nm wavelength.The 1inear range of iodine was 0.0001—0.002mol·L-1（r=0.9995）,the average recovery（n=9） was 99.48%.The method is convenient,accurate,reproducible and suitable for the quality control of Povidone iodine solution. |
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| Keywords: | Spectrophotometry Povidone Iodine Iodine |
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