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Reassignment of the structures of condensation products of α-keto α′-formylarylhydrazones with ethyl cyanoacetate: a novel route to ethyl 5-arylazo-2-hydroxynicotinates
Authors:Saleh M Al-Mousawi  Moustafa Sherief Moustafa  Ismail Abdelshafy Abdelhamid  Mohamed Hilmy Elnagdi
Institution:a Department of Chemistry, Faculty of Science, University of Kuwait, PO Box 12613, Safat 13060, Kuwait
b Institut für Organische Chemie der Universität Hannover, Schneiderberg 1B, 30167 Hannover, Germany
c Chemistry Department, Faculty of Science, Cairo University Giza, Egypt
Abstract:The condensation of α-keto α′-formylarylhydrazones with ethyl cyanoacetate afforded ethyl 5-arylazo-2-hydroxy-6-aryl (or alkyl) nicotinates. The structures of the reaction products could be established based on X-ray crystal structure determination.
Keywords:Arylhydrazonals  Condensation  Ethyl cyanoacetate  Ethyl 5-arylazo-2-hydroxynicotinate
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