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大豆天然甾醇的提取
引用本文:谢兵,傅相锴,隋岩,曾仁权.大豆天然甾醇的提取[J].西南师范大学学报(自然科学版),2005,30(5):897-900.
作者姓名:谢兵  傅相锴  隋岩  曾仁权
作者单位:1. 西南大学,化学化工学院,重庆,400715
2. 西南大学,化学化工学院,重庆,400715;西南大学,荣昌校区基础部,重庆,402460
摘    要:用皂化法研究了7种不同原料中大豆甾醇的提取量,实验表明大豆油脱臭馏出物(简称DD油))是大豆箱醇提取的理想原料,对皂化法从DD油中提取大豆甾醇的实验条件进行正交优化,最佳实验条件是:400gDD油,500mL乙醇(95%),50gKOH(82%),回流皂化2h.在此条件下.粗甾醇的产量为26.0g,纯度为47.5%.

关 键 词:大豆油脱臭馏出物  皂化  提取  天然大豆甾醇
文章编号:1000-5471(2005)05-0897-04
收稿时间:2004-11-26
修稿时间:2004年11月26

Extracting of Natural Soybean Phytosterol
XIE Bing,FU Xiang-kai,SUI Yan,ZENG Ren-quan.Extracting of Natural Soybean Phytosterol[J].Journal of Southwest China Normal University(Natural Science),2005,30(5):897-900.
Authors:XIE Bing  FU Xiang-kai  SUI Yan  ZENG Ren-quan
Institution:1. School of Chemistry and Chemical Engineering, Southwest University, Chongqing 400715, China; 2. Basic Department of Rongchang Campus, Southwest University, Chongqing 402460, China
Abstract:The extracting yields of natural soybean phytosterol by means of saponification from seven different raw materials was investigated. It is indicated with the experimental results, that the soybean oil deodorizer distillate (DD oil) is the best ideal material of extracting of soybean phytosterol. The optimum experimental conditions of extracting soybean phytosterol from DD oil by means of saponification were explored with orthogonal experiments. The optimum experimental conditions were that 50 g of potassium hydroxide (82%) was dropped into the solution of 400 g of DD oil in 500 ml ethanol (95%), and the mixture was refluxed for 2 hours. Under such conditions, 26 g of crude soybean phytosterol was obtained, and its purity was about 47.5%.
Keywords:soybean oil deodorizer distillate (DD oil)  saponification  extraction  natural soybean phytosterol
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