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Quantification of the pore size distribution (porosity profiles) in microfiltration membranes by SEM,TEM and computer image analysis
Authors:R. Ziel  A. Haus  A. Tulke
Affiliation:1. Mainsite GmbH & Co. KG, Analytical Services Obernburg, Industrie Center Obernburg, D-63784 Obernburg, Germany;2. Polyamide High Performance GmbH, Industrie Center Obernburg, D-63784 Obernburg, Germany
Abstract:Transport properties of membranes are closely related to morphological properties like surface porosity and variation of their inner pore structure. Scanning electron microscopy (SEM) as well as transmission electron microscopy (TEM) are powerful tools to characterise the microscopical pore structure of membranes in a qualitative manner. In order to provide more quantitative data of surface and cross-sectional pores computer image analysis can be used. Parameters like ‘porous area fraction’ and ‘mean free path length’ have been selected to describe the pore distribution within porosity profiles in order to consider the effect that the pores within the cross-section are connected to each other.
Keywords:Microfiltration membrane   Computer image analysis   Scanning electron microscopy   Transmission electron microscopy   Porosity profiles
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