Micellar chromatographic separation of vanadium(V) chelate with 2-(2-thiazolylazo)-5-dimethylaminophenol |
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Authors: | Jun''ichiro Miura |
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Affiliation: | (1) Department of Applied Chemistry and Biotechnology, Fukui University, Bunkyo-3, 910 Fukui, Japan |
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Abstract: | Summary In reversed phase—high performance liquid chromatography for metal chelates with 2-(2-thiazolylazo)-5-dimethylaminophenol, an aqueous non-ionic surfactant solution is used as a mobile phase. Among V(V), Fe(III), Cu(II), Co(II), Ni(II), Cd(II), Zn(II), Mn(II), and Al(III), only the V(V) chelate gave a resolved peak by using 0.8% w/w poly(oxyethylene)n-4-nonylphenyl ether (n=20) solution buffered at pH 3.8. V(V) can be selectively separated and sensitively determined. |
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