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Trace elemental characterization of edible oils by ICP-AES and GFAAS
Authors:Iva Juranovic Cindric  Ilse Steffan
Institution:a Laboratory of Analytical Chemistry, Faculty of Science, University of Zagreb, Horvatovac 102 a, HR-10000 Zagreb, Croatia
b Institute of Analytical Chemistry, University of Vienna, Währingerstraβe 38, A-1090 Vienna, Austria
Abstract:A method for the determination of the inorganic profile in edible oils is proposed. The quantification of selected metals in various oils (olive, pumpkin seed, sunflower, sesame seed, hazelnut, grape, soya, rice oil) was carried out using microwave assisted digestion followed by ICP-AES and GFAAS. The detection power of the ICP-AES technique was sufficient for the determination of Ca, Fe, Mg, Na, and Zn. Since the samples contained very low amounts of Al, Cu, Co, Cr, K, Ni, Mn, and Pb, these elements were measured by GFAAS. Differences of metal concentrations for edible oils obtained in this preliminary study represent a starting basis for the development of an additional analytical procedure applicable for oil characterization.
Keywords:Edible oils  Trace elements  Characterization  ICP-AES  GFAAS
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