| Microwave Assisted Synthesis of 3,3',3″,3'″-o-,p-Phenylenedi-methylidinetetrakis-(4-hydroxy-2H-1-benzopyran-2-one) |
| |
| 基金项目： | Supported by the National Natural Science Foundation of China(No.20672091). |
| |
| 摘 要： | Under microwave irradiation,2,2'-alkoxy-bridging or 4,4'-alkoxy-bridging dibenzaldehydes reacted with 4-hydroxycoumarin in DMF to give a series of 3,3',3″,3'″-o-and 3,3',3″,3'″-p-phenylenedimethylidinetetrakis-(4-hydroxy-2H-1-benzopyran-2-ones) in moderate yields.The structures of the synthetic coumarin derivatives were characterized with IR,1H NMR and MS spectroscopy as well as X-ray single crystallography.
|
| 收稿时间： | 2010-01-21 |
Microwave Assisted Synthesis of 3,3',3″,3'″-o-, p-Phenylenedi-methylidinetetrakis-(4-hydroxy-2H-1-benzopyran-2-one) |
| |
| Authors: | AN Lin LIU Dong-mei WANG Jin-xiang and YAN Chao-guo |
| |
| Institution: | 1. College of Pharmacy, Xuzhou Medical College, Xuzhou 221004, P. R. China;
2. College of Chemistry & Chemical Engineering, Yangzhou University, Yangzhou 225002, P. R. China |
| |
| Abstract: | Under microwave irradiation, 2,2'-alkoxy-bridging or 4,4'-alkoxy-bridging dibenzaldehydes reacted with 4-hydroxycoumarin in DMF to give a series of 3,3',3″,3'″-o- and 3,3',3″,3'″-p-phenylenedimethylidinetetrakis-(4- hydroxy-2H-1-benzopyran-2-ones) in moderate yields. The structures of the synthetic coumarin derivatives were characterized with IR, 1H NMR and MS spectroscopy as well as X-ray single crystallography. |
| |
| Keywords: | Microwave irradiation One-pot reaction Coumarin Benzopyran-2-one |
| 本文献已被 CNKI 万方数据 等数据库收录！ |
| 点击此处可从《高等学校化学研究》浏览原始摘要信息 |
| 点击此处可从《高等学校化学研究》下载免费的PDF全文 |
|
