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微波消解ICP-AES法测定植株金属元素含量的研究
引用本文:张昕,赵永和,张巍松. 微波消解ICP-AES法测定植株金属元素含量的研究[J]. 河南科学, 2005, 23(5): 675-678
作者姓名:张昕  赵永和  张巍松
作者单位:黄淮学院化学化工系,河南,驻马店,463000;中国石油大学,北京,102249
基金项目:河南省科技攻关计划项目(0424270130)
摘    要:植株金属元素含量是农田环境质量评价中的必检项目.微波消解ICP-AES法测定植株金属元素含量具有分析速度快,线性范围宽等优点.研究了微波消解ICP-AES法测定植株样品中包括K、Ca、Mg、Cu、Zn、Fe、Mn、Al、Cd、Cr、Mo、P、Pb、S、Si等15种元素的检测条件和检测限以及测定中的不定误差,为植株样品中金属元素含量的ICP检测提供了理论依据.

关 键 词:植株  金属元素含量  微波消解  ICP-AES法  检测限  误差
文章编号:1004-3918(2005)05-0675-04
收稿时间:2005-04-01
修稿时间:2005-04-01

The study of metals in plant samples and its error estimation with microwave digestion and ICP-AES
ZHANG Xin,ZHAO Yong-he,ZHANG Wei-song. The study of metals in plant samples and its error estimation with microwave digestion and ICP-AES[J]. Henan Science, 2005, 23(5): 675-678
Authors:ZHANG Xin  ZHAO Yong-he  ZHANG Wei-song
Abstract:The mass and trace metal element contents in the plant had to be measured in grade estimation of farm enviroment. Microwave digestion and ICP-AES were dsed to analyze the heavy meatl elements in the plant. The method had many advantages such as high analytical speed and broad linear range etc. The detection limit of fifteen masss and trace meatal elements inclading K, Ca, Mg,Cu,Zn, Fe, Mn, Al, Cd, Cr, Mo, P, Pb, S, and, Si in the plant and the uncertain error estimation during the measuring were studided by using microwave digestion and ICP-AES. Which supplide the theoretical foundation for the measure determination of metal elements in many plant samples.
Keywords:plant  mental element content  microwave digestion  ICP-AES  detection limit  error
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