| Synthesis and characterization of α-N,N-dihydroxyethylaminopropyl-ω-butylpolydimethylsiloxanes |
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| 作者姓名： | Yi Tao Yu Qing Si Zhang Meng Zhang Hai Feng Sun |
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| 作者单位： | a School of Chemical Engineering, Shandong Institute of Light Industry, Jinan 250100, China;b School of Chemistry and Material, Southern Yangtz University, Wuxi 214122, China |
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| 基金项目： | We gratefully acknowledge the financial support of the Natural Science Foundation of Shandong Province （No. Y2006B22）. |
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| 摘 要： | A series of α-N,N-dihydroxyethylaminopropyl-ω-butylpolydimethylsiloxanes with different molecular weight were synthesized. The preparation included five steps which were hydroxyl protection, alkylation, anionic ring-opening polymerization, hydrosilylation and deprotection. The structure of reaction products was characterized by FT-IR, GC, 1H NMR. 2007 Qing Si Zhang. Published by Elsevier B.V. on behalf of Chinese Chemical Society. All rights reserved.
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| 关 键 词： | 羟基保护 合成 烷化作用 阴离子开环聚合 氢化硅烷化 |
| 收稿时间： | 11 September 2007 |
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