| 卤代苯和卤代萘磺化产物的1H NMR研究 |
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| 引用本文： | 邹友思,林静.卤代苯和卤代萘磺化产物的1H NMR研究[J].波谱学杂志,1996,13(1):61-68. |
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| 作者姓名： | 邹友思 林静 |
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| 作者单位： | 厦门大学化学系, 厦门 361005 |
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| 基金项目： | 国家教委回国人员科研经费资助 |
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| 摘 要： | 研究了卤代苯和卤代萘磺化产物的1H NMR分析方法.结合各产物有关质子的化学位移,偶合常数,分裂形式,积分高度可得到各种磺化产物的比例.讨论了双共振去偶合实验的具体应用,化学位移理论值的计算及其在质子谱峰归属中所起的作用,磺化产物1H和19F的偶合分裂现象.首次报道了卤代芳香化合物多磺酸取代产物的1H NMR数值.
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| 关 键 词： | 核磁共振 磺化反应 卤代苯 卤代萘 |
| 收稿时间： | 1995-04-14 |
1H NMR STUDY ON THE SULFO DERIVATIVES OF HALOBENZENES AND HALONAPHTHALENES |
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| Zou Yousi and Lin Jing.1H NMR STUDY ON THE SULFO DERIVATIVES OF HALOBENZENES AND HALONAPHTHALENES[J].Chinese Journal of Magnetic Resonance,1996,13(1):61-68. |
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| Authors: | Zou Yousi and Lin Jing |
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| Institution: | Department of Chemistry, Xiamen University, Xiamen 361005 |
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| Abstract: | H NMR study on the reaction products of sulfur trioxide with four halobenzenes, six halonaphthalenes is reported. The chemical shifts of sulfo derivatives have been assigned. The 1H NMR data of disulfo and trisulfo derivatives of halobenzenes and halonaphthalenes have been reported for the first time. The application of double resonance, coupling constant of 1H and 19F, calculation data of chemical shift were also discussed. |
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| Keywords: | H NMR Sulfo-derivative Halobenzene Halonaphthalene |
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