| 三重四级杆气相色谱–串联质谱联用仪的校准 |
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| 引用本文： | 赵迎晨,冯帅博,李琛,李佳. 三重四级杆气相色谱–串联质谱联用仪的校准[J]. 化学分析计量, 2016, 0(5): 104-107. DOI: 10.3969/j.issn.1008-6145.2016.05.027 |
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| 作者姓名： | 赵迎晨 冯帅博 李琛 李佳 |
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| 作者单位： | 河南省计量科学研究院化学计量研究所,郑州,450008 |
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| 基金项目： | 河南省质量技术监督局科技计划项目(编号2015zj22) |
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| 摘 要： | 参考JJF 1164–2006《台式气相色谱–质谱联用仪校准规范》,探讨了三重四级杆气相色谱–串联质谱联用仪的校准方法,提出了以分辨力、定性定量重复性、检出限、质量准确性与谱库检索等5项作为相关校准项目。经验证,用该校准方法对三重四级杆气相色谱–串联质谱联用仪进行校准是可行的。
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| 关 键 词： | 气相色谱-质谱联用仪 三重四级杆 检出限 校准方法 |
Calibration Techniques for Triple Quadrupole Gas Chromatography-Mass Spectrometer |
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| Abstract: | The calibration method of GC–MS/MS instrument was discussed. The calibration items such as resolution, qualitative and quantitative repeatability, detection limit, quality accuracy and spectral library search were proposed referring to JJF1164 –2006 Calibration Specification for Bench Top Gas Chromatography–Mass Spectrometers. The method was used to calibrate GC–MS/MS and it is proved that the method is reasonable. |
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| Keywords: | gas chromatography-mass spectrometry triple quadrupole detection limit calibration method |
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