Efficient Synthesis of 3,5,6,8-Tetrahydro-4H-thiopyrano[4',3':4,5]thieno[2,3-d]pyrimidin-4-ones via an Iminophosphorane |
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Authors: | LI Wen-jing LIU Min FENG Ling-ling DING Ming-wu |
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Abstract: | 3,5,6,8-Tetrahydro-4H-thiopyrano[4',3':4,51thieno[2,3-d]pyrimidin-4-ones(7) were synthesized via the base catalytic reactions of amines or phenols with carbodiimides(5),which were obtained from the aza-Wittig reactions of iminophosphoranes(4) with aromatic isocyanates. |
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Keywords: | 3,5,6,8-Tetrahydro-4H-thiopyrano[4',3':4,5]thieno[2,3-d]pyrimidin-4-one Aza-Wittig reaction Carbodii-mide Isocyanate |
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