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Efficient Synthesis of 3,5,6,8-Tetrahydro-4H-thiopyrano[4',3':4,5]thieno[2,3-d]pyrimidin-4-ones via an Iminophosphorane
Authors:LI Wen-jing  LIU Min  FENG Ling-ling  DING Ming-wu
Abstract:3,5,6,8-Tetrahydro-4H-thiopyrano4',3':4,51thieno2,3-d]pyrimidin-4-ones(7) were synthesized via the base catalytic reactions of amines or phenols with carbodiimides(5),which were obtained from the aza-Wittig reactions of iminophosphoranes(4) with aromatic isocyanates.
Keywords:3  5  6  8-Tetrahydro-4H-thiopyrano[4'  3':4  5]thieno[2  3-d]pyrimidin-4-one  Aza-Wittig reaction  Carbodii-mide  Isocyanate
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