| 微波促进下9-芳基氢化吖啶-1,8-二酮的合成研究 |
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| 引用本文： | 薛载坤,张用伟,毛润泽,张新迎.微波促进下9-芳基氢化吖啶-1,8-二酮的合成研究[J].化学研究与应用,2012,24(1):101-105. |
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| 作者姓名： | 薛载坤 张用伟 毛润泽 张新迎 |
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| 作者单位： | 1. 河南师范大学化学与环境科学学院,河南新乡,453007
2. 河南师范大学化学与环境科学学院,河南新乡453007;河南化工职业学院化学工程系,河南郑州450042 |
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| 基金项目： | 河南省教育厅自然科学基金 |
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| 摘 要： | 本文研究了微波促进下芳香醛、5,5-二甲基-1,3-环己二酮与碳酸氢铵的三组分无溶剂缩合反应,并通过该反应合成了一系列9-芳基氢化吖啶-1,8-二酮类化合物.这一合成方法具有操作简便、反应条件温和、产率高、对环境友好等特点.
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| 关 键 词： | 9-芳基氢化吖啶-1 8-二酮 多组分反应 无溶剂反应 微波辐射 |
Preparation of 9-arylacridine-1,8-dione derivatives under MWI |
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| XUE Zai-kun
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ZHANG Yong-wei
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MAO Run-ze
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ZHANG Xin-ying.Preparation of 9-arylacridine-1,8-dione derivatives under MWI[J].Chemical Research and Application,2012,24(1):101-105. |
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| Authors: | XUE Zai-kun ZHANG Yong-wei MAO Run-ze ZHANG Xin-ying |
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| Institution: | 1*(1.College of Chemistry and Environmental Science,Henan Normal University,Xinxiang 453007,China; 2.Henan Industrial University Chemical Technology Vocational College,Zhengzhou 450042,China) |
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| Abstract: | A novel synthesis of 9-arylacridine-1,8-diones through a three-component reaction of aldehyde,5,5-dimethyl-1,3-cyclohexanedione and ammonium bicarbonate under microwave irradiation was presented.Advantages of this new synthetic protocol included easy operation,mild reaction conditions,high efficiency,and environmental benigncy. |
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| Keywords: | 9-Arylacridine-1 8-dione multi-component reaction solvent-free reaction microwave irradiation |
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