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沉淀双点滴定法测定盐酸左旋咪唑
引用本文:张云,夏海艳,高学鹏,李通化.沉淀双点滴定法测定盐酸左旋咪唑[J].分析试验室,2008,27(11).
作者姓名:张云  夏海艳  高学鹏  李通化
作者单位:同济大学化学系,上海,200092
摘    要:以Ag^+作滴定剂,分别用双点滴定法和传统电位滴定法对盐酸左旋咪唑片进行了测定。试液的配制采用了过滤和不过滤两种方法。测定结果表明:所有方法测得的结果均在《药典》允许的范围之内;本法测定结果与《药典》规定方法的对照偏差约为2%-3%;采用过滤和不过滤两种方法配制试液的测定结果之间的偏差约为1%。

关 键 词:盐酸左旋咪唑  双点滴定法  沉淀滴定  电位滴定

Determination of levamisole hydrochloride by precipitation double-point titrimetry
ZHANG Yun,XIA Hai-yan,GAO Xue-peng,LI Tong-hua.Determination of levamisole hydrochloride by precipitation double-point titrimetry[J].Chinese Journal of Analysis Laboratory,2008,27(11).
Authors:ZHANG Yun  XIA Hai-yan  GAO Xue-peng  LI Tong-hua
Abstract:According to the chinese pharmacopoeia the determination method for levamisole hydrochloride is non-aqueous titration.In this work,levamisole hydrochloride is determined by double-point titrimetry and traditional potentiometric titrimetry respectively using silver ion as the titrant in an aqueous solution.There are two kinds of test solution preparation,namely filtration and non-filtration. The determination results in this paper have the following features.Firstly,both analysis data got from double-point t...
Keywords:Levamisole hydrochloride  Double-point titrimetry  Precipitation titration  Potentiometric titration  
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