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Capillary headspace - gas chromatography for the characterization of the flavour of fresh vegetables
Authors:A. Shinohara  A. Sato  H. Ishii  N. Onda
Affiliation:(1) Central Research Laboratory, Takasago International Corporation, 36-31, 5-chome, Kamata, Ohta-ku, 114 Tokyo, Japan;(2) Perkin-Elmer Japan Co., Ltd., 8-4, 2-chome, Kitasaiwai, Nishi-ku, 220 Yokohama, Japan
Abstract:Summary Static headspace sampling combined with gas chromatography using open-tubular (capillary) columns for the characterization of the flavour of raw vegetables and some vegetable products is described. In order to avoid alteration of the composition of the volatiles, the sample was thermostated for a short time only. Although equilibrium between vapour and sample was not established the reproducibility of such conditions is demonstrated. Typical chromatograms are given; the most characteristic compounds present were identified by mass spectrometry. Enlarged text of a poster presented at the Twelfth International symposium on Capillary Chromatography, September 11–14, 1990, Kobe, Japan
Keywords:Gas chromatography  Non-equilibrium headspace sampling  Vegetables and food products  Flavour compounds
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