Some studies on thallium oxalates — IV |
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Authors: | S R Sagi Karri V Ramana M S Prasada Rao |
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Institution: | (1) Inorganic Chemistry Laboratories, Andhra University, Waltair, India |
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Abstract: | Thallium(III) was precipitated with oxalic acid in the presence of 0.025M RbNO3 (or 0.0125M Rb2SO4) in 0.1M HNO3 (or 0.05M H2SO4). Chemical analysis of the solid obtained corresponds to the formula RbTlIII(C2O4)2]·4 H2O. Thermal studies (TG, DTG and DTA) indicated the dehydration and redox decomposition of the thallic salt to the thallous salt, and finally to a mixture of rubidium carbonate and oxides of thallium(I) and thallium(III). Infrared absorption spectra, microscopic observations and X-ray diffraction data were used to characterize the original salt, as well as the intermediates formed during the thermal decomposition of the salt. On the basis of these results, the salt may be represented as: RbTlIII(C2O4)2(H2O)2]·2 H2O.
Zusammenfassung Thallium (III) wurde mit Oxalsäure in Gegenwart von 0.025M RbNO3 (oder 0.0125M Rb2SO4) in 0.1M HNO3 (oder 0.05M H2SO4) gefällt. Die chemische Analyse der erhaltenen Festsubstanz entspricht der Formel RbTlIII(C2O4)2]·4H2O. Thermische Untersuchungen (TG, DTG und DTA) zeigen die Dehydratisierung und Redoxzersetzung vom Thallitsalz zum Thallitsalz und schließlich zu einem Gemisch von Rubidiumcarbonat und Oxiden der Thallium(I) und Thallium(III). Infrarot-Absorptionsspektren, mikroskopische Beobachtungen und Röntgendiffraktionsdaten werden zur Charakterisierung des ursprünglichen Salzes sowie der während der thermischen Zersetzung des Salzes entstandenen Zwischenprodukte angewandt. Durch diese Ergebnisse kann das Salz wie folgt beschrieben werden: RbTlIII(C2O4)2(H2O)2]·2H2O.
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![gcy](/content/t8g88258733r4644/xxlarge1075.gif) ![rcy](/content/t8g88258733r4644/xxlarge1088.gif) ![acy](/content/t8g88258733r4644/xxlarge1072.gif) ![fcy](/content/t8g88258733r4644/xxlarge1092.gif) ![icy](/content/t8g88258733r4644/xxlarge1080.gif) ![chcy](/content/t8g88258733r4644/xxlarge1095.gif) ![iecy](/content/t8g88258733r4644/xxlarge1077.gif) ![scy](/content/t8g88258733r4644/xxlarge1089.gif) ![icy](/content/t8g88258733r4644/xxlarge1080.gif) ![dcy](/content/t8g88258733r4644/xxlarge1076.gif) ![acy](/content/t8g88258733r4644/xxlarge1072.gif) ![ncy](/content/t8g88258733r4644/xxlarge1085.gif) ![ncy](/content/t8g88258733r4644/xxlarge1085.gif) ![ycy](/content/t8g88258733r4644/xxlarge1099.gif) ![bcy](/content/t8g88258733r4644/xxlarge1073.gif) ![ycy](/content/t8g88258733r4644/xxlarge1099.gif) ![lcy](/content/t8g88258733r4644/xxlarge1083.gif) ![icy](/content/t8g88258733r4644/xxlarge1080.gif) ![scy](/content/t8g88258733r4644/xxlarge1089.gif) ![pcy](/content/t8g88258733r4644/xxlarge1087.gif) ![ocy](/content/t8g88258733r4644/xxlarge1086.gif) ![lcy](/content/t8g88258733r4644/xxlarge1083.gif) ![zcy](/content/t8g88258733r4644/xxlarge1079.gif) ![ocy](/content/t8g88258733r4644/xxlarge1086.gif) ![vcy](/content/t8g88258733r4644/xxlarge1074.gif) ![acy](/content/t8g88258733r4644/xxlarge1072.gif) ![ncy](/content/t8g88258733r4644/xxlarge1085.gif) ![dcy](/content/t8g88258733r4644/xxlarge1076.gif) ![lcy](/content/t8g88258733r4644/xxlarge1083.gif) ![khcy](/content/t8g88258733r4644/xxlarge1093.gif) ![acy](/content/t8g88258733r4644/xxlarge1072.gif) ![rcy](/content/t8g88258733r4644/xxlarge1088.gif) ![acy](/content/t8g88258733r4644/xxlarge1072.gif) ![kcy](/content/t8g88258733r4644/xxlarge1082.gif) ![tcy](/content/t8g88258733r4644/xxlarge1090.gif) ![iecy](/content/t8g88258733r4644/xxlarge1077.gif) ![rcy](/content/t8g88258733r4644/xxlarge1088.gif) ![icy](/content/t8g88258733r4644/xxlarge1080.gif) ![scy](/content/t8g88258733r4644/xxlarge1089.gif) ![tcy](/content/t8g88258733r4644/xxlarge1090.gif) ![icy](/content/t8g88258733r4644/xxlarge1080.gif) ![kcy](/content/t8g88258733r4644/xxlarge1082.gif) ![kcy](/content/t8g88258733r4644/xxlarge1082.gif) ![acy](/content/t8g88258733r4644/xxlarge1072.gif) ![acy](/content/t8g88258733r4644/xxlarge1072.gif) ![chcy](/content/t8g88258733r4644/xxlarge1095.gif) ![acy](/content/t8g88258733r4644/xxlarge1072.gif) ![lcy](/content/t8g88258733r4644/xxlarge1083.gif) ![softcy](/content/t8g88258733r4644/xxlarge1100.gif) ![ncy](/content/t8g88258733r4644/xxlarge1085.gif) ![ocy](/content/t8g88258733r4644/xxlarge1086.gif) ![scy](/content/t8g88258733r4644/xxlarge1089.gif) ![ocy](/content/t8g88258733r4644/xxlarge1086.gif) ![lcy](/content/t8g88258733r4644/xxlarge1083.gif) , ![tcy](/content/t8g88258733r4644/xxlarge1090.gif) ![acy](/content/t8g88258733r4644/xxlarge1072.gif) ![pcy](/content/t8g88258733r4644/xxlarge1087.gif) ![rcy](/content/t8g88258733r4644/xxlarge1088.gif) ![ocy](/content/t8g88258733r4644/xxlarge1086.gif) ![mcy](/content/t8g88258733r4644/xxlarge1084.gif) ![iecy](/content/t8g88258733r4644/xxlarge1077.gif) ![zhcy](/content/t8g88258733r4644/xxlarge1078.gif) ![ucy](/content/t8g88258733r4644/xxlarge1091.gif) ![tcy](/content/t8g88258733r4644/xxlarge1090.gif) ![ocy](/content/t8g88258733r4644/xxlarge1086.gif) ![ncy](/content/t8g88258733r4644/xxlarge1085.gif) ![ycy](/content/t8g88258733r4644/xxlarge1099.gif) ![pcy](/content/t8g88258733r4644/xxlarge1087.gif) ![rcy](/content/t8g88258733r4644/xxlarge1088.gif) ![ocy](/content/t8g88258733r4644/xxlarge1086.gif) ![dcy](/content/t8g88258733r4644/xxlarge1076.gif) ![ucy](/content/t8g88258733r4644/xxlarge1091.gif) ![kcy](/content/t8g88258733r4644/xxlarge1082.gif) ![tcy](/content/t8g88258733r4644/xxlarge1090.gif) ![ocy](/content/t8g88258733r4644/xxlarge1086.gif) , ![ocy](/content/t8g88258733r4644/xxlarge1086.gif) ![bcy](/content/t8g88258733r4644/xxlarge1073.gif) ![rcy](/content/t8g88258733r4644/xxlarge1088.gif) ![acy](/content/t8g88258733r4644/xxlarge1072.gif) ![zcy](/content/t8g88258733r4644/xxlarge1079.gif) ![yucy](/content/t8g88258733r4644/xxlarge1102.gif) ![shchcy](/content/t8g88258733r4644/xxlarge1097.gif) ![icy](/content/t8g88258733r4644/xxlarge1080.gif) ![khcy](/content/t8g88258733r4644/xxlarge1093.gif) ![scy](/content/t8g88258733r4644/xxlarge1089.gif) ![vcy](/content/t8g88258733r4644/xxlarge1074.gif) ![vcy](/content/t8g88258733r4644/xxlarge1074.gif) ![rcy](/content/t8g88258733r4644/xxlarge1088.gif) ![iecy](/content/t8g88258733r4644/xxlarge1077.gif) ![mcy](/content/t8g88258733r4644/xxlarge1084.gif) ![tcy](/content/t8g88258733r4644/xxlarge1090.gif) ![iecy](/content/t8g88258733r4644/xxlarge1077.gif) ![rcy](/content/t8g88258733r4644/xxlarge1088.gif) ![mcy](/content/t8g88258733r4644/xxlarge1084.gif) ![icy](/content/t8g88258733r4644/xxlarge1080.gif) ![chcy](/content/t8g88258733r4644/xxlarge1095.gif) ![iecy](/content/t8g88258733r4644/xxlarge1077.gif) ![scy](/content/t8g88258733r4644/xxlarge1089.gif) ![kcy](/content/t8g88258733r4644/xxlarge1082.gif) ![ocy](/content/t8g88258733r4644/xxlarge1086.gif) ![gcy](/content/t8g88258733r4644/xxlarge1075.gif) ![rcy](/content/t8g88258733r4644/xxlarge1088.gif) ![acy](/content/t8g88258733r4644/xxlarge1072.gif) ![zcy](/content/t8g88258733r4644/xxlarge1079.gif) ![lcy](/content/t8g88258733r4644/xxlarge1083.gif) ![ocy](/content/t8g88258733r4644/xxlarge1086.gif) ![zhcy](/content/t8g88258733r4644/xxlarge1078.gif) ![iecy](/content/t8g88258733r4644/xxlarge1077.gif) ![ncy](/content/t8g88258733r4644/xxlarge1085.gif) ![icy](/content/t8g88258733r4644/xxlarge1080.gif) ![scy](/content/t8g88258733r4644/xxlarge1089.gif) ![ocy](/content/t8g88258733r4644/xxlarge1086.gif) ![lcy](/content/t8g88258733r4644/xxlarge1083.gif) . ![Ocy](/content/t8g88258733r4644/xxlarge1054.gif) ![scy](/content/t8g88258733r4644/xxlarge1089.gif) ![ncy](/content/t8g88258733r4644/xxlarge1085.gif) ![vcy](/content/t8g88258733r4644/xxlarge1074.gif) ![ycy](/content/t8g88258733r4644/xxlarge1099.gif) ![vcy](/content/t8g88258733r4644/xxlarge1074.gif) ![acy](/content/t8g88258733r4644/xxlarge1072.gif) ![yacy](/content/t8g88258733r4644/xxlarge1103.gif) ![scy](/content/t8g88258733r4644/xxlarge1089.gif) ![ncy](/content/t8g88258733r4644/xxlarge1085.gif) ![ecy](/content/t8g88258733r4644/xxlarge1101.gif) ![tcy](/content/t8g88258733r4644/xxlarge1090.gif) ![icy](/content/t8g88258733r4644/xxlarge1080.gif) ![rcy](/content/t8g88258733r4644/xxlarge1088.gif) ![iecy](/content/t8g88258733r4644/xxlarge1077.gif) ![zcy](/content/t8g88258733r4644/xxlarge1079.gif) ![ucy](/content/t8g88258733r4644/xxlarge1091.gif) ![softcy](/content/t8g88258733r4644/xxlarge1100.gif) ![tcy](/content/t8g88258733r4644/xxlarge1090.gif) ![acy](/content/t8g88258733r4644/xxlarge1072.gif) ![tcy](/content/t8g88258733r4644/xxlarge1090.gif) ![acy](/content/t8g88258733r4644/xxlarge1072.gif) , ![scy](/content/t8g88258733r4644/xxlarge1089.gif) ![ocy](/content/t8g88258733r4644/xxlarge1086.gif) ![lcy](/content/t8g88258733r4644/xxlarge1083.gif) ![mcy](/content/t8g88258733r4644/xxlarge1084.gif) ![ocy](/content/t8g88258733r4644/xxlarge1086.gif) ![zhcy](/content/t8g88258733r4644/xxlarge1078.gif) ![iecy](/content/t8g88258733r4644/xxlarge1077.gif) ![bcy](/content/t8g88258733r4644/xxlarge1073.gif) ![ycy](/content/t8g88258733r4644/xxlarge1099.gif) ![tcy](/content/t8g88258733r4644/xxlarge1090.gif) ![pcy](/content/t8g88258733r4644/xxlarge1087.gif) ![rcy](/content/t8g88258733r4644/xxlarge1088.gif) ![iecy](/content/t8g88258733r4644/xxlarge1077.gif) ![dcy](/content/t8g88258733r4644/xxlarge1076.gif) ![scy](/content/t8g88258733r4644/xxlarge1089.gif) ![tcy](/content/t8g88258733r4644/xxlarge1090.gif) ![acy](/content/t8g88258733r4644/xxlarge1072.gif) ![vcy](/content/t8g88258733r4644/xxlarge1074.gif) ![iecy](/content/t8g88258733r4644/xxlarge1077.gif) ![ncy](/content/t8g88258733r4644/xxlarge1085.gif) ![vcy](/content/t8g88258733r4644/xxlarge1074.gif) ![icy](/content/t8g88258733r4644/xxlarge1080.gif) ![dcy](/content/t8g88258733r4644/xxlarge1076.gif) RbTl111(C2O4)2(H2O)2·2 2O.
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