Correlation between i.r. spectra and thermal decomposition of cobalt(II), nickel(II), copper(II) and mercury(II) complexes with piperidinedithiocarbamate and pyrrolidinedithiocarbamate |
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Authors: | Cavalheiro Éder T G Ionashiro Massao Marino Glimaldo Breviglieri Susete T Chierice Gilberto O |
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Institution: | (1) Depto. Química, UFSCar, São Carlos, São Paulo, CP 676, CEP 13565-905, Brazil;(2) Instituto de Química, UNESP, Araraquara, São Paulo, CP 355, CEP 14800-900, Brazil;(3) Inst. de Química de S. Carlos, USP, São Carlos, São Paulo, CP 780, CEP 13560-970, Brazil |
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Abstract: | The thermal decomposition of pyrrolidinedithiocarbamate and piperidinedithiocarbamate complexes of CoII, NiII, CuII and HgII have been studied by thermogravimetry and differential scanning calorimetry. The decomposition intermediates and final products were identified by their X-ray diffraction patterns. The i.r. spectra are discussed in terms of the thermal decomposition pathways. |
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