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Practical aspects of V and Nb solid-state NMR spectroscopy and applications to oxide materials

Authors:	OB Lapina DF Khabibulin VV Terskikh

Institution:	^a Boreskov Institute of Catalysis, Prosp. Lavrentieva 5, Novosibirsk 630090, Russia ^b Steacie Institute for Molecular Sciences, National Research Council Canada, Ottawa, Ont., Canada K1A 0R6

Abstract:

Keywords:	CP cross polarization CS chemical shielding CSA chemical shift anisotropy CT central transition CW continuous wave CW-NMR continuous wave nuclear magnetic resonance DAS dynamic-angle spinning DeNOx nitrogen oxide abatement DFT density functional theory DOR double rotation DQ double-quantum DQ STMAS double-quantum satellite transition magic-angle spinning EDAX energy dispersive X-ray spectroscopy EFG electric field gradient ESR electron spin resonance FID free induction decay FT-NMR Fourier transform nuclear magnetic resonance GIPAW gauge-including projected augmented-wave HETCOR heteronuclear correlation spectroscopy HFI hyperfine interaction tensor HFMAS high-field magic-angle spinning HREM high resolution electron microscopy HSMAS high-speed magic-angle spinning KTN KTa_(1&minus x)Nb_xO₃ MAS magic-angle spinning MASSA magic-angle spinning and static spectra analysis MQMAS multiple quantum magic-angle spinning MQ multiple quantum NMR nuclear magnetic resonance NQR nuclear quadrupolar resonance QCPMG quadrupolar Carr-Purcell Meiboom-Gill PBN Ba-substituted Pb(Mg_1/3Nb_2/3)O₃ PMN Pb(Mg_1/3Nb_2/3)O₃ PMN/PT (1&minus x)Pb(Mg_1/3Nb_2/3)O₃/xPbTiO₃ PSN Sc-substituted Pb(Mg_1/3Nb_2/3)O₃ PZN Zr-substituted Pb(Mg_1/3Nb_2/3)O₃ REAPDOR rotational echo adiabatic passage double resonance REDOR rotational echo double resonance RF radio frequency SATRAS satellite transition spectroscopy SBV Strongly bound vanadium SEDOR spin-echo double resonance ST satellite transition STMAS satellite transition magic-angle spinning SSTMAS spinning sidebands analysis of selected transitions TRAPDOR transfer of population in double resonance VOCS variable offset cumulative spectrum
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