L-lysine-Pd Complex Supported on Fe3O4 MNPs: a novel recoverable magnetic nanocatalyst for Suzuki C-C Cross-Coupling reaction |
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| Authors: | Muhammad Aqeel Ashraf Zhenling Liu Dangquan Zhang Ashkan Alimoradi |
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| Institution: | 1. School of Forestry, Henan Agricultural University, Zhengzhou, 450002 China
Department of Geology Faculty of Science, University of Malaya, Kuala Lumpur, 50603 Malaysia;2. School of Management, Henan University of Technology, Zhengzhou, 450001 China;3. School of Forestry, Henan Agricultural University, Zhengzhou, 450002 China;4. Department for Management of Science and Technology Development, Ton Duc Thang University, Ho Chi Minh City, Vietnam |
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| Abstract: | In this work, L-lysine-Pd Complex, immobilized onto the surface of Fe3O4 MNPs, was successfully prepared via simple and inexpensive procedure. The prepared nanocatalyst was considered as a robust and clean nano-reactor catalyst for the Suzuki and Heck C-C Cross-Coupling reactions in water as the green condition. This eco-friendly heterogeneous catalyst was characterized by Fourier transform infrared spectroscopy (FT-IR), X-Ray Diffractometer (XRD), energy-dispersive X-ray spectroscopy (EDS), inductively coupled plasma atomic emission spectroscopy (ICP), X-ray mapping, BET, thermogravimetric analysis (TGA), vibrating sample magnetometer (VSM), scanning electron microscopy (SEM) and Transmission electron microscopy (TEM) techniques. The use of a green medium, easy separation and workup, excellent reusability of the nanocatalyst and short reaction time are some outstanding advantages of this method. |
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| Keywords: | C-C coupling Fe3O4@L-lysine-Pd Nanocatalyst reusable catalyst Suzuki reaction |
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