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Analysis of precipitates in ultrafine-grained metallic materials
Authors:V.D. Sitdikov  R.K. Islamgaliev  M.A. Nikitina  G.F. Sitdikova  K. X. Wei  I.V. Alexandrov
Affiliation:1. Institute of Physics of Advanced Materials, Ufa State Aviation Technical University, Ufa, Russia;2. School of Materials Science and Engineering, Changzhou University, Changzhou, P.R. People's Republic of China;3. Sino-Russia Joint Laboratory of Functional Nanostructured Materials, Changzhou University, Changzhou, P.R. People's Republic of China;4. National Experimental Demonstration Center for Materials Science and Engineering, Changzhou University, Changzhou, P.R. People's Republic of China
Abstract:In the present work, new possibilities of the X-ray diffraction for investigations of the phase composition, size, shape and volume fraction of particles in ultrafine-grained ferritic/martensitic steel and the Cu-Cr-Zr alloy have been demonstrated. For the first time, the method of X-ray diffraction in the transmission mode was used to identify particles with a volume fraction of less than one percent in the ultrafine-grained materials studied. The small-angle X-ray scattering method was used to estimate the size and shape of dispersed particles. Specific features of the ultrafine-grained structure determined by the X-ray diffraction and transmission electron microscopy studies were used for estimation of dispersion hardening in the samples obtained by equal-channel angular pressing in comparison with the samples subjected to standard treatment.
Keywords:X-ray diffraction in transmitted mode  ferritic/martensitic steel  copper alloy  small-angle X-ray diffraction
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