New reaction of benzo[b]thieno[3,2-b]benzo[b]thiophene disulfone |
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Authors: | V. É. Udre É. Ya. Lukevits A. A. Kemme Ya. Ya. Bleidelis |
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Affiliation: | (1) Institute of Organic Synthesis, Academy of Sciences of the Latvian SSR, 226006 Riga |
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Abstract: | A new reaction of benzo[b]thieno[3,2-b]benzo[b]thiophene disulfone with amines that takes place with opening of one of the thiophene rings and nucleophilic substitution in the heteroaromatic ring at the site of cleavage of the S-C bond was observed. The molecular structures of the products of amination of the disulfone were determined by x-ray diffraction analysis. Hydrolysis and dehydration of the amination products gave derivatives of a new heterocyclic system, viz., benzo[b]-thieno[3,2-e]benzo[c]-1,2-oxathiin. Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 3, pp. 320–323, March, 1980. |
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