Synthesis and study of ammonium hexamolybdobismuthate(III) |
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Authors: | A. V. Oreshkina G. Z. Kaziev N. N. Lobanov A. V. Steblevskii |
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Affiliation: | 1.Moscow State Pedagogical University,Moscow,Russia;2.Russian University of Peoples’ Friendship,Moscow,Russia;3.Kurnakov Institute of General and Inorganic Chemistry,Russian Academy of Sciences,Moscow,Russia |
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Abstract: | Ammonium hexamolybdobismuthate(III) of composition (NH4)3[BiMo6O18(OH)6] · 7H2O (I) was synthesized and studied by mass spectrometry, X-ray diffraction, IR spectroscopy, and thermogravimetry. The compound is monoclinic: a = 10.438 Å, b = 7.909 Å, c = 18.127 Å, β = 96.59°, V = 1486.76 Å3, ρcalc = 3.32 g/cm3, Z = 2. |
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