| 高效液相色谱法测定卷烟烟气总粒相物中的烟碱 |
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| 引用本文： | 谢笑天,郑萍,朱伟明,赵革玲.高效液相色谱法测定卷烟烟气总粒相物中的烟碱[J].分析化学,2000,28(9):1085-1087. |
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| 作者姓名： | 谢笑天 郑萍 朱伟明 赵革玲 |
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| 作者单位： | 1. 云南师范大学化学系,昆明,650092
2. 云南省烟草质量监督检验站,昆明,650106 |
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| 基金项目： | 云南省政府与北京大学省校科技合作项目 |
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| 摘 要： | 采用反相高效液相色谱内标法测定卷烟烟气总粒相物中的烟碱含量，内标物为对氨基苯碘酸，方法的平行回收率为９９．７％～１００．１％，精密度好，操作简便、快速，可作为检测烟碱的一种可靠方法。
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| 关 键 词： | 烟碱 卷烟 总粒相物 高效液相色谱法 烟气 |
Separation and Determination of Nicotine in Total Particulate Matter of Cigarette Gas by High Performance Liquid Chromatography |
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| Xie Xiaotian,Zheng Ping,Zhu Weiming,Zhao Geling.Separation and Determination of Nicotine in Total Particulate Matter of Cigarette Gas by High Performance Liquid Chromatography[J].Chinese Journal of Analytical Chemistry,2000,28(9):1085-1087. |
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| Authors: | Xie Xiaotian Zheng Ping Zhu Weiming Zhao Geling |
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| Abstract: | A HPLC internal standard method has been developed to determine the concentration of nicotine in total particulate matter of cigarette gas. p-Aminobenzene sulfonic acid was used as the internal standard. The average recovery of method was 99. 7% - 100.1% and the RSD was 0.9%. The experiments showed that the method was accurate and reliable. |
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| Keywords: | Nicotine cigarette total peculate matter high performance liquid chromatography |
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