Bis(bis(trimethylsilyl)phosphino)silan [(Me3Si)2P]2SiH2 und 1,2-Bis(bis(trimethylsilyl)phosphino)disilan [(Me3Si)2PSiH2]2 |
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| Institution: | 1. Centro de Investigaciones Químicas, Universidad Autónoma del Estado de Hidalgo, km. 4.5 Carretera Pachuca-Tulancingo, Col. Carboneras, C.P. 42184 Mineral de la Reforma, Hidalgo, Mexico;2. Centro Conjunto de Investigación en Química Sustentable UAEM-UNAM, km 14.5 Carretera Toluca-Atlacomulco, Unidad San Cayetano, C.P. 50200 Toluca, Edo. de México, Mexico |
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| Abstract: | The compounds H2SiP(SiMe3)2]2 and H2SiP(SiMe3)2]2 were prepared and characterized by 29Si NMR, 31P NMR, IR and Raman spectroscopy. After thermolysis of these compounds no cyclic silylphosphanes could be detected in the reaction mixture,although this did contain P(SiMe3)3. |
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