| 芳香醛与硫代巴比妥酸的缩合反应研究 |
| |
| 引用本文： | 路军,李迎迎,杨玲,白银娟,田敏.芳香醛与硫代巴比妥酸的缩合反应研究[J].有机化学,2003,23(9):958-960. |
| |
| 作者姓名： | 路军 李迎迎 杨玲 白银娟 田敏 |
| |
| 作者单位： | 西北大学化学系,西安,710069 |
| |
| 基金项目： | 陕西省自然科学基金(No.2000H03)资助项目. |
| |
| 摘 要： | 通过微波辐射、用水作溶剂及在醋酸铵催化下的固相研磨等，研究了芳香醛与 硫代巴比妥酸的缩合反应。在三种反应条件下都得到了5-芳亚苄基硫代巴比妥酸， 并通过IR，~1H NMR和元素分析确定了产物的结构。
|
| 关 键 词： | 微波辐射 乙酸铵 芳亚苄基硫代巴比妥酸 缩合反应 红外分光光度法 质子磁共振谱法 元素分析 |
| 修稿时间： | 2003年11月12 |
Study on the Condensation Reactions between Aromatic Aldehydes and Thiobarbituric Acid |
| |
| LU,Jun LI,Ying-Ying YANG,Ling BAI,Yin-Juan TIAN,Min.Study on the Condensation Reactions between Aromatic Aldehydes and Thiobarbituric Acid[J].Chinese Journal of Organic Chemistry,2003,23(9):958-960. |
| |
| Authors: | LU Jun LI Ying-Ying YANG Ling BAI Yin-Juan TIAN Min |
| |
| Institution: | Department of Chemistry, Northwest University |
| |
| Abstract: | The condensation reactions between aromatic aldehydes and thiobarbituric acid were carried out under microwave irradiation, by grinding the reactants using NH 4OAc as a catalyst, or with heating in water to give 5-arylidene thiobarbituric acid. The structures of the condensation products were characterized by elemental analysis, IR and 1H NMR spectra. |
| |
| Keywords: | solid state grinding microwave irradiation 5-arylidene thiobarbituric acid |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
| 点击此处可从《有机化学》浏览原始摘要信息 |
| 点击此处可从《有机化学》下载免费的PDF全文 |
