| 微波消解-等离子体原子发射光谱法测定杨梅中的微量元素 |
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| 引用本文： | 王晓赛,沈燕,季小武,朱小琼,韩超.微波消解-等离子体原子发射光谱法测定杨梅中的微量元素[J].光谱实验室,2010,27(3):1002-1004. |
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| 作者姓名： | 王晓赛 沈燕 季小武 朱小琼 韩超 |
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| 作者单位： | 1. 温州大学化学与材料工程学院,浙江省温州市茶山高教园区,325035
2. 温州出人境检验检疫局,浙江省温州市,325027 |
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| 摘 要： | 采用微波消解-电感耦合等离子体原子发射光谱法(ICP-AES)测定杨梅中Fe、Mg、Ba、Cu、Al、Zn、Mn、Co8种微量元素,对样品的前处理条件进行了探讨,通过加标回收实验,验证了分析数据的可靠性,在最佳测定条件下,方法检出限为0.0005—0.0100g/mL,相对标准偏差≤2.8%,加标回收率为95.7%—105.1%。方法快速、简便、准确,适合常规分析。
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| 关 键 词： | 杨梅 微波消解 微量元素 电感耦合等离子体-原子发射光谱法 |
Determination of Trace Elements in Myrica Rubra Sieb et Zucc.by ICP-AES with Microwave Digestion |
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| WANG Xiao-Sai,SHEN Yan,JI Xiao-Wu,ZHU Xiao-Qiong,HAN Chao.Determination of Trace Elements in Myrica Rubra Sieb et Zucc.by ICP-AES with Microwave Digestion[J].Chinese Journal of Spectroscopy Laboratory,2010,27(3):1002-1004. |
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| Authors: | WANG Xiao-Sai SHEN Yan JI Xiao-Wu ZHU Xiao-Qiong HAN Chao |
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| Institution: | a(College of Chemistry and Materials Engineering,Wenzhou University,Wenzhou,Zhejiang 325035,P.R.China)a(Wenzhou Entry-Exit Inspection and Quarantine Bureau,Wenzhou,Zhejiang 325027,P.R.China) |
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| Abstract: | The determination of eight elements （Fe,Mg,Ba,Cu,Al,Zn,Mn,Co） in myrica rubra Sieb et Zucc. was carried out by ICP-AES.The myrica rubra Sieb et Zucc.sample was digested by microwave digestion technique.Under the optimal conditions,the detection limit is 0.0005—0.0100μg/mL,and the RSD≤2.8%.The recovery is in the range of 95.7%—105.1%.The experimental results show that the method is easy,rapid and accuracy. |
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| Keywords: | Myrica Rubra Sieb et Zucc Microwave Digestion Trace Elements ICP-AES |
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