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快速溶胶-凝胶法制备SrAl2O4:Eu^2+,Dy^3+绿色长余辉荧光粉及表征
引用本文:刘振,焦桓,杨菊香.快速溶胶-凝胶法制备SrAl2O4:Eu^2+,Dy^3+绿色长余辉荧光粉及表征[J].光谱实验室,2011,28(4):1954-1957.
作者姓名:刘振  焦桓  杨菊香
作者单位:1. 西安文理学院化学与化工系 西安市太白南路168号710065
2. 陕西师范大学化学与材料科学学院 西安市长安南路199号710062
基金项目:西安文理学院2008年中青年专业技术人员科研项目资助
摘    要:建立一种快速溶胶-凝胶法制备长余辉材料的方法。以柠檬酸,硝酸锶,硝酸铝及硝酸铕等为原料,实现了该法的快速制备过程。研究结果表明,通过改进可使该法制备铝酸锶长余辉材料的时间缩短至12h以内,X射线粉末衍射,扫描电镜,光谱分析等表明,使用该方法与传统溶胶-凝胶法制备的样品其性能基本一致。

关 键 词:溶胶-凝胶  铝酸锶  长余辉

Rapid Preparation and Characterization of Green Long Afterglow Phosphors SrAl2O4:Eu2+,Dy3+ by Sol-Gel Method
LIU Zhen,JIAO Huan,YANG Ju-Xiang.Rapid Preparation and Characterization of Green Long Afterglow Phosphors SrAl2O4:Eu2+,Dy3+ by Sol-Gel Method[J].Chinese Journal of Spectroscopy Laboratory,2011,28(4):1954-1957.
Authors:LIU Zhen  JIAO Huan  YANG Ju-Xiang
Institution:(Department of Chemistry & Cheraical Engineering, Xi' an University of Arts and Science, Xi' an 730065, P. R. China; aSchool of Chemistry and Materials Science,Shaanxi Normal University,Xi' an 710062 ,P. R. China)
Abstract:A method for the rapid preparation of green long afterglow phosphors SrAl2O4-Eu^2+,Dy^3+ was established. With citric acid, strontium nitrate, aluminum nitrate and europium nitrate,etc as raw materials,the rapid preparation was achieved. The time of preparation of long afterglow phosphors SrAl2O4: Eu^2+, Dy^3+ could be shorten the time to under 12 hours by improvement experiment. The synthesized products were characterized by X ray diffraction,scanning electron microscopy and spectrum analysis, etc. The prepared sample by the method is tended to be consistent with the traditional sol-gel method.
Keywords:Sol-Gel  SrAl2O4  Long Afterglow
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