| 大黄酸与锌配位反应的影响因素 |
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| 引用本文： | 黄超锋,陈燕,熊伟,胡欣怡,赵芳. 大黄酸与锌配位反应的影响因素[J]. 光谱实验室, 2011, 28(4): 1837-1840 |
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| 作者姓名： | 黄超锋 陈燕 熊伟 胡欣怡 赵芳 |
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| 作者单位： | 石河子大学化学化工学院化学系 新疆石河子市北四路832000 |
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| 基金项目： | 石河子大学大学生研究训练计划项目，国家自然科学基金 |
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| 摘 要： | 通过单因素试验和正交试验,系统研究了大黄酸与锌离子发生配位反应的影响因素。结果表明,大黄酸锌配合物合成的最佳条件：pH为9.0,反应温度为30℃,反应时间为80min。最佳条件验证实验最大产率为87.3%,采用红外光谱对配合物进行了表征。
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| 关 键 词： | 大黄酸 锌 配合物 |
Influencing Factors on Coordination Reaction Between Rhein and Zinc |
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| HUANG Chao-Feng,CHEN Yan,XIONG Wei,HU Xin-Yi,ZHAO Fang. Influencing Factors on Coordination Reaction Between Rhein and Zinc[J]. Chinese Journal of Spectroscopy Laboratory, 2011, 28(4): 1837-1840 |
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| Authors: | HUANG Chao-Feng CHEN Yan XIONG Wei HU Xin-Yi ZHAO Fang |
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| Affiliation: | (Department of Chemistry,College of Chemistry and Chemical Engineering,Shihezi University,Shihezi,Xinjiang 832000,P.R.China) |
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| Abstract: | The influencing factors on the reaction between rhein and zinc were investigated by single factor and orthogonal experiment.The optimal conditions were as follows： pH of 9.0,reaction temperature of 30℃ and reaction time for 80min.Under optimal conditions,the yield of the complex was 87.3%.The structure of the complex was characterized by IR spectrum. |
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| Keywords: | Rhein Zinc Complex |
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