Factors affecting reproducibility in the manufacture of glass and siliceous glass open tubular (capillary) columns |
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Authors: | W G Jennings R H Wohleb R G Jenkins |
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Institution: | (1) Department of Food Science and Technology, University of California, 95616 Davis, CA, U.S.A.;(2) J & W Scientific, Inc., 95670 Rancho Cordova, CA, U.S.A. |
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Abstract: | Summary Column characteristics affecting the chromatographic behavior of glass and siliceous glass ( fused silica ) capillary columns include the dimensional uniformity of the column, the physical and chemical characteristics of the column wall and the characteristics of the liquid phase. In the case of the coated column the uniformity and thickness of the liquid phase film are the most important criteria affecting column reproducibility. The paper discusses these factors and their influence on column performance.Presented in part at the Symposium on Standardized Materials for Chromatography, 181 st National American Chemical Society Meeting, Atlanta, Georgia, March 29–April 3, 1981. |
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Keywords: | Gas chromatography Open tubular (capillary) columns Glass columns Fused-silica columns Column testing |
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