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X-ray and carbon-13 nuclear magnetic resonance characterization of cyclopropane derivatives obtained by solvolysis of (E)-3α- and (E)-3β-hydroxy-5,10-seco-1(10)-cholesten-5-one tosylates |
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| Authors: | Mihailo Lj Mihailović Ljubinka Lorenc Milan Dabović Ivan Juranić Ernest Wenkert Jean-Marie Bernassau Muppala S Raju Andrew T McPhail Richard W Miller |
| Institution: | Department of Chemistry, Faculty of Science, University of Belgrade, Studentski trg 16, 11000 Belgrade, Yugoslavia, and Institute of Chemistry, Technology and Metallurgy, Belgrade, Yugoslavia;Department of Chemistry, Rice University, Houston, Texas 77001, U. S. A.;Paul M. Gross Chemical Laboratory, Duke University, Durham, Nort Carolina 27706, U. S. A. |
| Abstract: | The stereochemistries and conformations of the cyclopropane ring containing compounds derived from (E-3α- and (E)-3β-hydroxy-5,10-seco-1(10)-cholesten-5-one tosylates have been determined by X-ray methods and the results correlated with 13C nmr chemical shift data. |
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