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The use of the capillary rheometer for the rheological evaluation of extrudable cement-based materials
Authors:Roberta Alfani  Nino Grizzuti  Gian Luca Guerrini  Gianluca Lezzi
Affiliation:(1) CTG Italcementi Group, Via G. Camozzi 124, 24121 Bergamo, Italy;(2) Dipartimento di Ingegneria Chimica, Università degli Studi di Napoli Federico II, P.le Tecchio 80, 80125 Naples, Italy
Abstract:In this paper, the rheological properties of an extrudable cement-based paste are investigated by means of an original ram extrusion apparatus (capillary rheometer). The experimental results indicate that a careful measurement of the die pressure is necessary to obtain a realistic viscosity vs shear rate curve, as required in extrusion technology. In particular, it is shown that the optimal test configuration is when the pressure measurement is made directly inside the rheometer die. By applying this rheological methodology in steady-state conditions, it has been observed that the extrudable cement-based material here evaluated obeys to a simple power–law equation, in the range of shear rates investigated, which are suitable for an industrial extrusion process. This paper was presented at the third Annual European Rheology Conference (AERC) held in Hersonissos, Crete, Greece, April 24–27, 2006.
Keywords:Cement paste  Capillary rheometry  Slit die
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