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| 微波辐射下水相中3,5-双亚苄基哌啶-4-酮衍生物的合成 | |
| 引用本文： | 彭菊花,韩正国,郝文娟,曹旭东,石枫. 微波辐射下水相中3,5-双亚苄基哌啶-4-酮衍生物的合成[J]. 有机化学, 2009, 29(8): 1228-1231 |
| 作者姓名： | 彭菊花 韩正国 郝文娟 曹旭东 石枫 |
| 作者单位： | 1. 连云港师范高等专科学校化学系,连云港,222006 2. 徐州师范大学化学化工学院,徐州,221116 |
| 基金项目： | 国家自然科学基金，江苏省自然科学基金，江苏省六大人才高峰 |
| 摘 要： | 利用微波辐射, 以碳酸钾为催化剂, 快速于水相中合成了一系列3,5-双亚苄基哌啶-4-酮衍生物, 所合成化合物的结构经红外光谱、核磁共振光谱和高分辨率质谱予以确证. |
| 关 键 词： | 1-取代哌啶-4-酮 双亚苄基哌啶-4-酮物 微波辐射 |
| 收稿时间： | 2008-11-23 |
| 修稿时间： | 2009-01-20 |
Synthesis of 3,5-Bis(benzylidene)piperidin-4-one Derivatives in Water under Microwave Irradiation |
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| Peng Juhua,Han Zhengguo,Hao Wenjuan,Cao Xudong,Shi Feng. Synthesis of 3,5-Bis(benzylidene)piperidin-4-one Derivatives in Water under Microwave Irradiation[J]. Chinese Journal of Organic Chemistry, 2009, 29(8): 1228-1231 | |
| Authors: | Peng Juhua Han Zhengguo Hao Wenjuan Cao Xudong Shi Feng |
| Affiliation: | (a Department of Chemistry, Lianyungang Teachers’ College, Lianyungang 222006) (b School of Chemistry and Chemical Engineering, Xuzhou Normal University, Xuzhou 221116) |
| Abstract: | A series of 3,5-bis(benzylidene)piperidin-4-one derivatives were successfully synthesized through a rapid reaction in water catalyzed by K2CO3 under microwave irradiation, and structurally characterized by IR, 1H NMR and HRMS techniques. |
| Keywords: | 1-substituted-piperidin-4-one bis(benzylidene)piperidin-4-one microwave irradiation |
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