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Synthesis of analogs of 5(4)-aminoimidazole-4(5)-caeboxamide and purines
Authors:V I Ofitserov  Z S Mokrushin  Z V Pushkareva  N V Nikiforova
Institution:(1) S. M. Kirov Ural Polytechnic Institute, Sverdlovsk
Abstract:4(5)-Sulfonyl chlorides, which were converted to the corresponding sulfamoyl derivatives, were obtained from the amide and ethyl ester of 4(5)-mercaptoimidazole-5(4)-carboxylic acid by oxidative chlorination. The azide of 4(5)-sulfamoylimidazole-5(4)carboxylic acid was synthesized through 4(5)-sulfamoylimidazole-5(4)-carboxylhydrazide, and its conversion in various media to 5(4)-aminoimidazole-4(5)-sulfonamide derivatives and to 3,4-dihydro-3-oxoimidazo4,5-e]-1,2,4-thiadiazine 1,1-dioxide was studied.See 1] for communication V.Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 8, pp. 1119–1122, August, 1976.
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