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中红外光谱透射比标准物质研制
引用本文:冯国进,马宇轩,梁凤臣,甘海勇,郑春弟,吴厚平,张巧香,刘子龙.中红外光谱透射比标准物质研制[J].化学分析计量,2020,29(1):1-3.
作者姓名:冯国进  马宇轩  梁凤臣  甘海勇  郑春弟  吴厚平  张巧香  刘子龙
作者单位:中国计量科学研究院,北京100013;中国计量科学研究院,北京100013;中国计量科学研究院,北京100013;中国计量科学研究院,北京100013;中国计量科学研究院,北京100013;中国计量科学研究院,北京100013;中国计量科学研究院,北京100013;中国计量科学研究院,北京100013
摘    要:采用物化性质稳定的单晶硅作为基质,以直流磁控溅射方式轻蒸镀不同厚度的镍、铬混合膜层,实现了中红外波段(500~4000 cm^–1)不同透射比标准物质的研制。研制的中红外光谱透射比标准物质其透射比标称值分别为10%和50%,扩展不确定度优于0.008(k=2)。该标准物质具有量值稳定、光谱平坦等特点,可用于各类傅里叶变换红外光谱设备的透射比校准。

关 键 词:透射比  单晶硅  中红外光谱  标准物质

Preparation of mid-infrared transmittance standard reference materials
FENG Guojin,MA Yuxuan,LIANG Fengchen,GAN Haiyong,ZHENG Chundi,WU Houping,ZHANG Qiaoxiang,LIU Zilong.Preparation of mid-infrared transmittance standard reference materials[J].Chemical Analysis And Meterage,2020,29(1):1-3.
Authors:FENG Guojin  MA Yuxuan  LIANG Fengchen  GAN Haiyong  ZHENG Chundi  WU Houping  ZHANG Qiaoxiang  LIU Zilong
Institution:(National Institute of Metrology,Beijing 100013,China)
Abstract:Based on single crystal silicon substrate with stable physical and chemical properties,a series of transmittances in mid-infrared wave range of 500–4000 cm^–1 were achieved by coated with different thicknesses of Ni and Cr mixed film layers.The nominal values of the developed reference materials were 10%and 50%,respectively,and the expand uncertainty was better than 0.008(k=2).The reference material has the characteristics of stable value and flat spectrum,which can be used for the transmittance calibration of various Fourier transform infrared spectroscopy equipment.
Keywords:transmittance of material  single crystal silicon  mid-infrared spectroscopy  reference material
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