Synthesis and Crystal Structure of N-Methyl-9-(3,4-dimethoxylphenyl)-1,8-dioxo-1,2,3,4,5,6,7,8,9,10- decahydroacridine under Microwave Irradiation |
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| Authors: | ZHANG Xiao-Jing TU Shu-Jiang ZHU Xiao-Tong ZHANG Jin-Peng XU Jia-Ning WANG Qian |
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| Affiliation: | Department of Chemistry,Xuzhou Normal University;Key Lab of Biotechnology for Medicinal Plants of Jiangsu Province,Xuzhou,Jiangsu 221009,China;Department of Chemistry,Xuzhou Normal University;Key Lab of Biotechnology for Medicinal Plants of Jiangsu Province,Xuzhou,Jiangsu 221009,China;Department of Chemistry,Xuzhou Normal University;Key Lab of Biotechnology for Medicinal Plants of Jiangsu Province,Xuzhou,Jiangsu 221009,China;Department of Chemistry,Xuzhou Normal University;Key Lab of Biotechnology for Medicinal Plants of Jiangsu Province,Xuzhou,Jiangsu 221009,China;Department of Chemistry,Xuzhou Normal University;Key Lab of Biotechnology for Medicinal Plants of Jiangsu Province,Xuzhou,Jiangsu 221009,China;Department of Chemistry,Xuzhou Normal University;Key Lab of Biotechnology for Medicinal Plants of Jiangsu Province,Xuzhou,Jiangsu 221009,China |
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| Abstract: | The crystal structure of the title compound (C26H33NO4 (C25.68H32.04No.68O4.32, Mr =419.35)) has been determined by single-crystal X-ray diffraction. The crystal is of triclinic, space P21/c with a = 7.519(2), b = 28.933(5), c = 10.654(3) (A), β = 91.78(2)°, V= 2316.7(7) (A)3, Z = 4, Dc= 1.202 g/cm3,μ = 0.081 mm-1, F(000) = 902, Mr = 423, the final R = 0.0424 and wR = 0.0911. In the structure, the pyridine ring adopts a boat conformation. |
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| Keywords: | acridine microwave crystal structure |
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