Nitration of furan derivatives with acetyl nitrate |
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| Authors: | D O Lolya K K Venter É É Liepin'sh S A Giller |
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| Institution: | 1. Institute of Organic Synthesis, Academy of Science of the Latvian SSR, Riga
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| Abstract: | The mixture of products formed in the nitration of methyl furan-2-carboxylate in acetic anhydride was separated by means of thin-layer and column chromatography. It was found that products of cis and trans addition of acetyl nitrate to the furan ring — methyl 5-nitro-2-ace-toxy-2,5-dihydrofuran-2-carboxylate and 5-nitro-4-acetoxy-4,5-dihydrofuran-2-carboxylate — and methyl 5-nitrofuran-2-carboxylate are formed in the nitration. |
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