Spectroscopic characterization of copper(II) complexes of indoxyl N(4)-methyl thiosemicarbazone |
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| Authors: | Chandra Sulekh Kumar Umendra |
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| Institution: | Department of Chemistry, Zakir Husain College, University of Delhi, J.L. Nehru Marg, New Delhi 110002, India. schandra_00@yahoo.com |
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| Abstract: | New copper(II) complexes of indoxyl thiosemicarbazone (ITSC) of general composition CuL2X2 (where L: ITSC; X: Cl-, NO3-, ClO4-, NCS-) have been synthesized and characterized by elemental analysis, molar conductance, magnetic susceptibility measurements and spectral (electronic, IR, EPR, 1H NMR, Mass) studies. Cyclic voltammetry measurements show quasi-reversible Cu2+/Cu1+ couple. Various physico-chemical techniques suggest a tetragonal structure for these copper(II) complexes. |
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